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4. Signal intensities
Next to the number of signals in an NMR spectrum and their chemical
shifts, additional information about the compound in question can also
be derived from the intensities of the signals.
Please repeat:
- The intensity is measured as the
below
the resonance signal. To determine the area, the spectrum is integrated
automatically, and the cummulative integral is plotted on the spectrum.
- The intensities are proportional to the
,
that contribute to the signal.
As an example serves the spectrum of :
Above the spectrum the integral is plotted in red. The magnitude of the
steps in this curve is a direct representation of the number of protons
that contribute to each signal.
Assign the the protons in the molecule based on the integrals
of the signals (I) through (IV)
If you need some extra help, check on page 54!
If you want to compare your answer to the correct one, continue
to page 59 |
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